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Downstream Asher


Developed and produced by ibss Group in cooperation with the inventor of a unique, patented plasma source, the GV10x is the new generation in situ Downstream Asher. Competitively priced, the GV10x Downstream Asher reduces carbon & hydrocarbon contamination 10 to 20 times more effectively than traditional methods at vacuum pressures safe for turbo molecular pump (TMP) operation. Artifacts in SEM images are gone; the microscope maintains high resolution and beam stability. Black scan squares are eliminated in SEM images. Carbon contamination in FIB and TEM systems can be controlled as well.

Highlights:

  • Power  - 5 to 99 Watts continuously adjustable plasma power.
  • Pressure - 2 Torr to <5 mTorr (measured at the Source)
    • At higher pressure (>50 mTorr), the mean free path of the cleaning gas is short, allowing for decontamination in regions near the source.
    • At lower pressure (<50 mTorr), the longer mean free path of the cleaning gas allows for uniform carbon contamination removal. Also, the cleaning occurs at pressures safe for TMP operation
  • Gentle - ashes gas phase hydrocarbons and surface carbon by non-kinetic process with either neutral oxygen or hydrogen radicals

The GV10x, when coupled to the Gentle Asher™ Chamber, can clean specimens prior to examination. Reports from customers claim that this combination mitigates carbon on TEM holders/specimens and SEM samples with less damage and at less than ½ the cost of typical 'plasma cleaners'.

The GV10x Downstream (DS) Asher is the new paradigm in situ cleaner for vacuum chambers. The GV10x reduces carbon & hydrocarbons ~10 to 20 times more effectively & uniformly than first generation methods with the delicate DS process. The Turbo Molecular Pump (TMP) can be operated safely without interrupting the software control for SEM, FIB or TEM systems.


Typically the GV10x DS Asher uses air or oxygen gas to create oxygen radicals that remove hydrocarbon contamination.  Additionally, results from NIST show that using hydrogen gas in the GV10x DS Asher is safe and effective at removing carbon deposits on multilayer mirrors and other substrates and samples sensitive to oxidation. The ibss Group GV10x DS Ashercan be easily moved between several different laboratory instruments. Cleaning periods vary from chamber to chamber. The DS process, frequently called the remote plasma process, does not produce kinetic impingement, sputter damage, or sample heating, unlike usual plasma cleaners.  The GV10x DS Asher can quickly clean samples inside an SEM, allowing for rapid turnaround of artifact removal, typically in just a few minutes, without venting the microscope chamber.

The ibss Group Gentle Asher with a GV10x and pump extends the Downstream process to pre-clean specimens and TEM holders prior to insertion into the EM, increasing the time between microscope cleans. 

The GV10x is a new paradigm for cleaning chambers.  The process more quickly and with greater cleaning uniformity removes carbon contamination on surfaces in the far corners of a vacuum chamber that can constantly desorb and then recontaminate the rest of chamber.  Greater choice of power and pressure has allowed the GV10x to be applied, in addition to SEM chambers, to clean synchrotron and EUV optics, CDSEMs, Review SEMs and XPS systems where large chambers need to be cleaned uniformly and rapidly.

ibss Group, Inc. introduced the Gentle Asher to extend the GV10x investment to cleaning specimens before insertion into the EM chamber.  The Gentle Asher™ Chamber with a GV10x connected, GA/GV, is well suited for preventing black scan square buildup.

After de-contaminating an EM chamber to acceptable HC levels, one can utilize the DS process for sample cleaning and storage by simply moving the GVx Source onto the Gentle Asher Chamber. Reports from customers claim this cost effective combination delicately removes contamination from TEM holders and any type sample with less damage while keeping HC levels manageable in CDSEM, SEM, FIB and TEM.  Pre-cleaning samples and holders prevents contaminating the chamber gas phase that prolongs time between microscope cleanings.

The GV10x Downstream Asher’s ability to remove carbon contamination is a quantum leap beyond the traditional methods of mitigating contamination using cold trapping, nitrogen purging, and other plasma cleaners. The GV10x, with its extended power and pressure range (5 to 100 Watts and 2 to <0.005 Torr), represents a paradigm shift in the carbon decontamination of SEMs and other vacuum systems.

Atomic oxygen and hydrogen eliminates contamination by converting the surface carbon into gas phase molecules which are then pumped out of chambers - not just immobilized on trapping surfaces.  Sample artifacts such as polymerized deposits are minimized by low carbon levels in SEM chambers.

 

Since cleaning periods will vary between instruments, the GV10x DS Asher can be used on several laboratory tools by moving the GV10x Source from instrument to instrument.  Relocation of the GV10x DS Asher can be facilitated by placing an isolation valve between the GV10x Source and the instrument vacuum chamber, as seen on the S-4700 FESEM.

         

As nanoscience progresses, electron beams become more tightly focused, electron beam energies decrease, and precursor gas use increases, high resolution will become increasingly more dependent on keeping carbon contamination at low levels.  De-contamination and anti-contamination by remote or downstream plasma process accomplishes this task quickly, easily, and in a cost-effective way.  Unlike kinetic sputter etch cleaning in usual 'plasma cleaners', the downstream plasma process is a gentle chemical etch.  The process has revolutionized the means to eliminate carbon molecules and hydrocarbons in vacuum chambers. 

 

Well suited for large volume chambers and heavily contaminated surfaces, the GV10x DS Asher takes less time to achieve pristinely cleaned chambers, since it develops higher atomic oxygen and hydrogen concentrations to remove contamination with the same delicate result but in less time. Customers say that, ‘…using the GV10x we can achieve efficient and uniform hydrocarbon control throughout large chambers in 1/10 of the time’ and with more uniformity than with established methods’.

               

        



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